Information card for entry 7043069

Structure parameters

• Formula: C31 H56 Fe Ge O2 Si3
• Calculated formula: C31 H55 Fe Ge O2 Si3
• Title of publication: An Iron Germylene Complex Having Fe-H and Ge-H Bonds: Synthesis, Structure and Reactivity
• Authors of publication: Dhungana, Tara Prasad; Hashimoto, Hisako; Tobita, Hiromi
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 8.9028 ± 0.0005 Å
• b: 25.0183 ± 0.0011 Å
• c: 15.9058 ± 0.0006 Å
• α: 90°
• β: 91.6874 ± 0.0014°
• γ: 90°
• Cell volume: 3541.2 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0825
• Residual factor for significantly intense reflections: 0.0635
• Weighted residual factors for significantly intense reflections: 0.1053
• Weighted residual factors for all reflections included in the refinement: 0.1108
• Goodness-of-fit parameter for all reflections included in the refinement: 1.164
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No