Information card for entry 7043297

Structure parameters

• Formula: C28 H29 Cl3 N P2 Re
• Calculated formula: C28 H29 Cl3 N P2 Re
• Title of publication: Synthesis and Characterization of Rhenium(III) Complexes with (Ph2PCH2CH2)2NR Diphosphinoamine Ligands
• Authors of publication: Salvarese, Nicola; Refosco, Fiorenzo; Seraglia, Roberta; Roverso, Marco; Dolmella, Alessandro; Bolzati, Cristina
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 15.9425 ± 0.0003 Å
• b: 14.9601 ± 0.0003 Å
• c: 25.6721 ± 0.0006 Å
• α: 90°
• β: 103.822 ± 0.002°
• γ: 90°
• Cell volume: 5945.5 ± 0.2 ų
• Cell temperature: 300 ± 3 K
• Ambient diffraction temperature: 300 ± 3 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0389
• Residual factor for significantly intense reflections: 0.0236
• Weighted residual factors for significantly intense reflections: 0.047
• Weighted residual factors for all reflections included in the refinement: 0.0537
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No