Information card for entry 7043345

Structure parameters

• Chemical name: tetrabutylammonium tetra(phenylselenolato)oxidotechnetate(V) CH2Cl2 solvate
• Formula: C41 H58 Cl2 N O Se4 Tc
• Calculated formula: C41 H58 Cl2 N O Se4 Tc
• Title of publication: Technetium Complexes with Arylselenolato and Aryltellurolato Ligands
• Authors of publication: Noschang Cabral, Bruno; Kirsten, Lars; Hagenbach, Adelheid; Piquini, Paulo Cesar; Patzschke, Michael; Lang, Ernesto; Abram, Ulrich
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 15.4526 ± 0.0008 Å
• b: 18.3197 ± 0.0011 Å
• c: 15.7324 ± 0.0008 Å
• α: 90°
• β: 90.029 ± 0.002°
• γ: 90°
• Cell volume: 4453.6 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0409
• Residual factor for significantly intense reflections: 0.0349
• Weighted residual factors for significantly intense reflections: 0.0867
• Weighted residual factors for all reflections included in the refinement: 0.0907
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No