Information card for entry 7043436

Structure parameters

• Formula: C54 H56 N4 Ni O7.5 U
• Calculated formula: C54 H56 N4 Ni O7.5 U
• Title of publication: A versatile route to homo- and hetero-bimetallic 5f‒5f and 3d‒5f complexes supported by a redox active ligand framework
• Authors of publication: Camp, Clément; Toniolo, Davide; Andrez, Julie; Pécaut, Jacques; Mazzanti, Marinella
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 26.2314 ± 0.0008 Å
• b: 12.9229 ± 0.0003 Å
• c: 27.192 ± 0.0007 Å
• α: 90°
• β: 96.858 ± 0.003°
• γ: 90°
• Cell volume: 9151.7 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0855
• Residual factor for significantly intense reflections: 0.0467
• Weighted residual factors for significantly intense reflections: 0.0741
• Weighted residual factors for all reflections included in the refinement: 0.0846
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No