Information card for entry 7043530

Structure parameters

• Formula: C52 H55 Au Cl O4 P
• Calculated formula: C52 H55 Au Cl O4 P
• Title of publication: Calix[4]arene-fused phospholes
• Authors of publication: Elaieb, Fethi; Sémeril, David; Matt, Dominique; Pfeffer, Michel; Bouit, Pierre-Antoine; Hissler, Muriel; Gourlaouen, Christophe; Harrowfield, Jack
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 9.0854 ± 0.0009 Å
• b: 18.1789 ± 0.0019 Å
• c: 13.8937 ± 0.0015 Å
• α: 90°
• β: 99.456 ± 0.002°
• γ: 90°
• Cell volume: 2263.5 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0808
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.0756
• Weighted residual factors for all reflections included in the refinement: 0.0825
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No