Information card for entry 7043559

Structure parameters

• Formula: C16 H18 N8 Ni O2
• Calculated formula: C16 H18 N8 Ni O2
• Title of publication: Metal-mediated Reactions between Dialkylcyanamides and Acetamidoxime Generate Unusual (Nitrosoguanidinate)Nickel(II) Complexes
• Authors of publication: Bikbaeva, Zarina M.; Novikov, Alexander S.; Suslonov, Vitalii V.; Bokach, Nadezhda A.; Kukushkin, Vadim Yu.
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 6.5902 ± 0.0004 Å
• b: 11.1021 ± 0.0007 Å
• c: 12.3601 ± 0.0008 Å
• α: 90.489 ± 0.005°
• β: 95.586 ± 0.005°
• γ: 101.506 ± 0.005°
• Cell volume: 881.58 ± 0.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0799
• Residual factor for significantly intense reflections: 0.0607
• Weighted residual factors for significantly intense reflections: 0.1503
• Weighted residual factors for all reflections included in the refinement: 0.1604
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No