Information card for entry 7043576

Structure parameters

• Formula: C32 H34 B Cl8 N3 Ni P2
• Calculated formula: C32 H34 B Cl8 N3 Ni P2
• Title of publication: Triaminoborane-bridged diphosphine complexes with Ni and Pd: coordination chemistry, structures, and ligand-centered reactivity
• Authors of publication: Lee, Kyounghoon; Donahue, Courtney M.; Daly, Scott R.
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 9.9895 ± 0.001 Å
• b: 12.223 ± 0.0012 Å
• c: 16.8174 ± 0.0017 Å
• α: 90.04 ± 0.005°
• β: 103.664 ± 0.005°
• γ: 106.259 ± 0.005°
• Cell volume: 1910.6 ± 0.3 ų
• Cell temperature: 190 ± 2 K
• Ambient diffraction temperature: 190.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0458
• Residual factor for significantly intense reflections: 0.0318
• Weighted residual factors for significantly intense reflections: 0.0743
• Weighted residual factors for all reflections included in the refinement: 0.0823
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No