Information card for entry 7043916

Structure parameters

• Formula: C22 H21 Co N2 O3
• Calculated formula: C22 H21 Co N2 O3
• Title of publication: Flexibility and lability of a phenyl ligand in hetero-organometallic 3d metal-Sn(IV) compounds and their catalytic activity in Baeyer‒Villiger oxidation of cyclohexanone
• Authors of publication: Hazra, Susanta; Martins, Nuno M. R.; Kuznetsov, Maxim L.; Guedes da Silva, M. Fátima C.; Pombeiro, Armando J. L.
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 18.206 ± 0.002 Å
• b: 14.737 ± 0.0017 Å
• c: 6.7877 ± 0.0008 Å
• α: 90°
• β: 90.123 ± 0.001°
• γ: 90°
• Cell volume: 1821.1 ± 0.4 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0707
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.0846
• Weighted residual factors for all reflections included in the refinement: 0.092
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No