Information card for entry 7044006

Structure parameters

• Formula: C28 H36 N2 Si
• Calculated formula: C28 H36 N2 Si
• Title of publication: Ring Expansion of a Ring Expanded Carbene
• Authors of publication: Hill, Michael; Dutton, Jason Laurence; Wilson, David John; Mahon, Mary F.; Garcia, Lucia; Al Furaiji, Khalidah
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 13.268 ± 0.0003 Å
• b: 15.1828 ± 0.0003 Å
• c: 13.277 ± 0.0003 Å
• α: 90°
• β: 108.9 ± 0.003°
• γ: 90°
• Cell volume: 2530.39 ± 0.11 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0873
• Residual factor for significantly intense reflections: 0.0791
• Weighted residual factors for significantly intense reflections: 0.2242
• Weighted residual factors for all reflections included in the refinement: 0.2308
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No