Information card for entry 7044068

Structure parameters

• Formula: C13 H20 Cl2 N5 O Pd0.5
• Calculated formula: C13 H20 Cl2 N5 O Pd0.5
• Title of publication: Synthesis and redox reactions of bis(verdazyl) palladium complexes
• Authors of publication: Sanz, Corey A.; McKay, Zach R.; Patrick, Brian O.; MacLean, Shaun W.C.; Hicks, Robin G.
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 14.3982 ± 0.0019 Å
• b: 8.6271 ± 0.0012 Å
• c: 14.4349 ± 0.0019 Å
• α: 90°
• β: 107.688 ± 0.003°
• γ: 90°
• Cell volume: 1708.3 ± 0.4 ų
• Cell temperature: 90 K
• Ambient diffraction temperature: 90 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0288
• Residual factor for significantly intense reflections: 0.0236
• Weighted residual factors for significantly intense reflections: 0.0559
• Weighted residual factors for all reflections included in the refinement: 0.0584
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No