Information card for entry 7044128

Structure parameters

• Formula: C22 H52 Fe N8
• Calculated formula: C22 H52 Fe N8
• SMILES: [Fe]123([N](C)(CC[N]1(C)C)C)([N](=NN3CCCC)C(C)(C)C)[N](=NN2CCCC)C(C)(C)C
• Title of publication: Asymmetrically substituted triazenes as poor electron donor ligands in the precursor chemistry of iron(II) for iron-based metallic and intermetallic nanocrystals
• Authors of publication: Soussi, Khaled; Mishra, Shashank; Jeanneau, Erwann; Millet, Jean-Marc M; Daniele, Stephane
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 19.647 ± 0.001 Å
• b: 16.484 ± 0.002 Å
• c: 8.9926 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2912.4 ± 0.5 ų
• Cell temperature: 250 K
• Ambient diffraction temperature: 250 K
• Number of distinct elements: 4
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.135
• Residual factor for significantly intense reflections: 0.1143
• Weighted residual factors for all reflections: 0.2574
• Weighted residual factors for significantly intense reflections: 0.2187
• Weighted residual factors for all reflections included in the refinement: 0.2574
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9885
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No