Information card for entry 7044347

Structure parameters

• Formula: C108.5 H65 B2 F47 N4 P
• Calculated formula: C108.495 H65.04 B2 F46.99 N4 P
• Title of publication: Synthesis and Oxidation of Phosphine Cations†
• Authors of publication: Mehta, Meera; Johnstone, Tim; Lam, Jolie; Bidraha, Bid; Hermannsdorfer, Andre; Driess, Matthias; Stephan, Douglas W.
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 15.5736 ± 0.0004 Å
• b: 17.498 ± 0.0005 Å
• c: 18.9275 ± 0.0004 Å
• α: 83.61 ± 0.002°
• β: 89.0867 ± 0.0019°
• γ: 73.915 ± 0.003°
• Cell volume: 4924.6 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0815
• Residual factor for significantly intense reflections: 0.0699
• Weighted residual factors for significantly intense reflections: 0.1983
• Weighted residual factors for all reflections included in the refinement: 0.2143
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No