Information card for entry 7044386

Structure parameters

• Formula: C72.02 H116.62 Li2 O6.01 P2
• Calculated formula: C72.0212 H116.625 Li2 O6.0053 P2
• Title of publication: Desolvation and aggregation of sterically demanding alkali metal diarylphosphides
• Authors of publication: Izod, Keith; Evans, Peter; Waddell, Paul G.
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 11.32606 ± 0.00019 Å
• b: 17.4145 ± 0.0005 Å
• c: 19.3933 ± 0.0005 Å
• α: 68.346 ± 0.003°
• β: 80.5527 ± 0.0018°
• γ: 89.5652 ± 0.0018°
• Cell volume: 3501.07 ± 0.17 ų
• Cell temperature: 150 ± 0.2 K
• Ambient diffraction temperature: 150 ± 0.2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0534
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.097
• Weighted residual factors for all reflections included in the refinement: 0.1047
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No