Information card for entry 7044739

Structure parameters

• Formula: C14 H20 Cs4 Mo5 O24 P2
• Calculated formula: C14 H14 Cs4 Mo5 O24 P2
• Title of publication: Syntheses and characterization of phosphonates and diphosphonates of molybdenum, A4[(MoO3)5(O3PR)2]·xH2O, A2[Mo2O5(O3PR)2] and A2[Mo2O5(O3P-R-PO3)] (A = K, Rb, Cs, Tl, NH4)
• Authors of publication: Elias Jesu Packiam, D.; Vidyasagar, Kanamaluru
• Journal of publication: Dalton Transactions
• Year of publication: 2017
• a: 10.5867 ± 0.0002 Å
• b: 11.4057 ± 0.0002 Å
• c: 15.5112 ± 0.0003 Å
• α: 80.974 ± 0.001°
• β: 86.49 ± 0.001°
• γ: 76.21 ± 0.001°
• Cell volume: 1795.89 ± 0.06 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0548
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.1156
• Weighted residual factors for all reflections included in the refinement: 0.1201
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No