A Gel Aging Effect in the Synthesis of Open-Framework Gallium Phosphates: Structure Solution and Solid-State NMR of a Large-Pore, Open-Framework Material
Authors of publication
Broom, Lucy; Clarkson, Guy J.; Guillou, Nathalie; Hooper, Joseph; Dawson, Daniel; Tang, Chiu; Ashbrook, Sharon Elizabeth; Walton, Richard I.
Journal of publication
Dalton Transactions
Year of publication
2017
a
10.226818 ± 0.000063 Å
b
12.095846 ± 0.000071 Å
c
13.867132 ± 0.000081 Å
α
104.653 ± 0.0004°
β
100.811 ± 0.0006°
γ
102.523 ± 0.00062°
Cell volume
1565.84 ± 0.018 Å3
Cell temperature
293 K
Ambient diffraction temperature
293 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor R(I) for significantly intense reflections