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Information card for entry 7044996
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Coordinates | 7044996.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | [K(crypt-222)][(Tbb)GeBr2] |
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Chemical name | Tbb-germylemoid |
Formula | C45 H88 Br2 Ge K N2 O6 Si4 |
Calculated formula | C45 H88 Br2 Ge K N2 O6 Si4 |
Title of publication | 1,2-Dihalodigermenes bearing bulky Eind groups: synthesis, characterization, and conversion to halogermylenoids. |
Authors of publication | Hayakawa, Naoki; Sugahara, Tomohiro; Numata, Yasuyuki; Kawaai, Hotaka; Yamatani, Kenta; Nishimura, Shogo; Goda, Shun; Suzuki, Yuko; Tanikawa, Tomoharu; Nakai, Hidetaka; Hashizume, Daisuke; Sasamori, Takahiro; Tokitoh, Norihiro; Matsuo, Tsukasa |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2018 |
Journal volume | 47 |
Journal issue | 3 |
Pages of publication | 814 - 822 |
a | 11.8021 ± 0.0002 Å |
b | 12.4235 ± 0.0003 Å |
c | 20.4661 ± 0.0004 Å |
α | 79.322 ± 0.001° |
β | 78.119 ± 0.001° |
γ | 85.935 ± 0.001° |
Cell volume | 2884 ± 0.1 Å3 |
Cell temperature | 103 K |
Ambient diffraction temperature | 103 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0943 |
Residual factor for significantly intense reflections | 0.0872 |
Weighted residual factors for significantly intense reflections | 0.2161 |
Weighted residual factors for all reflections included in the refinement | 0.22 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.2 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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