Information card for entry 7045335

Structure parameters

• Formula: C30 H23 Cl3 F6 N2 O Pd
• Calculated formula: C30 H23 Cl3 F6 N2 O Pd
• Title of publication: The contradictory effect of the methoxy-substituent in palladium-catalyzed ethylene/methyl acrylate cooligomerization.
• Authors of publication: Rosar, V.; Meduri, A.; Montini, T.; Fornasiero, P.; Zangrando, E.; Milani, B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 8
• Pages of publication: 2778 - 2790
• a: 15.55 ± 0.002 Å
• b: 19.5 ± 0.002 Å
• c: 20.14 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6107 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0791
• Residual factor for significantly intense reflections: 0.0741
• Weighted residual factors for significantly intense reflections: 0.201
• Weighted residual factors for all reflections included in the refinement: 0.2049
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.7 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No