Information card for entry 7045707

Structure parameters

• Formula: C56 H74 B2 F10 P2
• Calculated formula: C56 H74 B2 F10 P2
• Title of publication: Formation and reactions of active five-membered phosphane/borane frustrated Lewis pair ring systems.
• Authors of publication: Dong, Shunxi; Wang, Long; Wang, Tongdao; Daniliuc, Constantin G.; Brinkkötter, Melanie; Eckert, Hellmut; Kehr, Gerald; Erker, Gerhard
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 13
• Pages of publication: 4449 - 4454
• a: 10.6253 ± 0.0005 Å
• b: 10.6747 ± 0.0005 Å
• c: 12.3972 ± 0.0006 Å
• α: 103.882 ± 0.002°
• β: 97.692 ± 0.002°
• γ: 100.679 ± 0.002°
• Cell volume: 1317.76 ± 0.11 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0754
• Residual factor for significantly intense reflections: 0.0643
• Weighted residual factors for significantly intense reflections: 0.1639
• Weighted residual factors for all reflections included in the refinement: 0.1709
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No