Information card for entry 7045902

Structure parameters

• Formula: C20 H50 Cl2 O4 P4 Pd2
• Calculated formula: C20 H50 Cl2 O4 P4 Pd2
• Title of publication: Synthesis and coordination chemistry of enantiopure t-BuMeP(O)H.
• Authors of publication: Gallen, Albert; Orgué, Sílvia; Muller, Guillermo; Escudero-Adán, Eduardo C; Riera, Antoni; Verdaguer, Xavier; Grabulosa, Arnald
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 15
• Pages of publication: 5366 - 5379
• a: 7.4353 ± 0.0005 Å
• b: 17.0371 ± 0.001 Å
• c: 12.4919 ± 0.0008 Å
• α: 90°
• β: 90.4112 ± 0.0019°
• γ: 90°
• Cell volume: 1582.38 ± 0.17 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.047
• Residual factor for significantly intense reflections: 0.0457
• Weighted residual factors for significantly intense reflections: 0.106
• Weighted residual factors for all reflections included in the refinement: 0.1066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.169
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No