Information card for entry 7045924

Structure parameters

• Formula: C26.75 H37 Cl N3 Pd Sb
• Calculated formula: C25 H35 Cl N3 Pd Sb
• Title of publication: Synthesis and non-conventional structure of square-planar Pd(ii) and Pt(ii) complexes with an N,C,N-chelated stibinidene ligand.
• Authors of publication: Kořenková, Monika; Hejda, Martin; Štěpnička, Petr; Uhlík, Filip; Jambor, Roman; RůŽička, Aleš; Dostál, Libor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 16
• Pages of publication: 5812 - 5822
• a: 10.406 ± 0.0011 Å
• b: 15.333 ± 0.0008 Å
• c: 18.462 ± 0.002 Å
• α: 76.301 ± 0.008°
• β: 75.302 ± 0.009°
• γ: 88.858 ± 0.007°
• Cell volume: 2765.7 ± 0.5 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0768
• Residual factor for significantly intense reflections: 0.0473
• Weighted residual factors for significantly intense reflections: 0.1035
• Weighted residual factors for all reflections included in the refinement: 0.1209
• Goodness-of-fit parameter for all reflections included in the refinement: 1.146
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No