Information card for entry 7045967

Structure parameters

• Formula: C9 H46 Ni3 O91 P2 Re3 W15
• Calculated formula: C9 Ni3 O91 P2 Re3 W15
• Title of publication: Immobilization of carbonyl rhenium tripods on the surface of a trinickel-substituted Dawson-type polyoxotungstate.
• Authors of publication: Jia, Jiage; Ma, Pengtao; Zhang, Panpan; Zhang, Dongdi; Zhang, Chao; Niu, Jingyang; Wang, Jingping
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 18
• Pages of publication: 6288 - 6292
• a: 14.5956 ± 0.0007 Å
• b: 22.3215 ± 0.0011 Å
• c: 14.8504 ± 0.0007 Å
• α: 90°
• β: 91.11 ± 0.001°
• γ: 90°
• Cell volume: 4837.3 ± 0.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0588
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.0994
• Weighted residual factors for all reflections included in the refinement: 0.11
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No