Information card for entry 7045984

Structure parameters

• Formula: C18 H75 Ge3 N18 Ni3 O45 Sb3 V15
• Calculated formula: C18 H72 Ge3 N18 Ni3 O45 Sb3 V15
• Title of publication: Ordnung muss sein: heteroelement order and disorder in polyoxovanadates.
• Authors of publication: Wendt, M.; Mahnke, L. K.; Näther, C; van Leusen, J.; Kögerler, P; Bensch, W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 19
• Pages of publication: 6672 - 6674
• a: 18.1983 ± 0.0012 Å
• b: 22.7116 ± 0.0015 Å
• c: 14.4488 ± 0.001 Å
• α: 90°
• β: 126.6 ± 0.006°
• γ: 90°
• Cell volume: 4794.3 ± 0.7 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 8
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0375
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.075
• Weighted residual factors for all reflections included in the refinement: 0.0775
• Goodness-of-fit parameter for all reflections included in the refinement: 0.996
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No