Crystallography Open Database

Information card for entry 7045998

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Structure parameters

Formula	C48 H54 K N O3 Si2
Calculated formula	C48 H54 K N O3 Si2
Title of publication	Salt metathesis routes to homoleptic near-linear Mg(ii) and Ca(ii) bulky bis(silyl)amide complexes.
Authors of publication	Leng, Ji-Dong; Goodwin, Conrad A. P.; Vitorica-Yrezabal, Iñigo J; Mills, David P.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	36
Pages of publication	12526 - 12533
a	11.7633 ± 0.0008 Å
b	12.7083 ± 0.0007 Å
c	17.4748 ± 0.0011 Å
α	70.553 ± 0.005°
β	75.294 ± 0.006°
γ	62.99 ± 0.007°
Cell volume	2178.2 ± 0.3 Å³
Cell temperature	150.02 ± 0.1 K
Ambient diffraction temperature	150.02 ± 0.1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0855
Residual factor for significantly intense reflections	0.0576
Weighted residual factors for significantly intense reflections	0.1276
Weighted residual factors for all reflections included in the refinement	0.147
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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