Information card for entry 7046000

Structure parameters

• Formula: C72 H60 Mg N2 Si4
• Calculated formula: C72 H60 Mg N2 Si4
• Title of publication: Salt metathesis routes to homoleptic near-linear Mg(ii) and Ca(ii) bulky bis(silyl)amide complexes.
• Authors of publication: Leng, Ji-Dong; Goodwin, Conrad A. P.; Vitorica-Yrezabal, Iñigo J; Mills, David P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 36
• Pages of publication: 12526 - 12533
• a: 13.9967 ± 0.0004 Å
• b: 13.9967 ± 0.0004 Å
• c: 14.5303 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2846.6 ± 0.16 ų
• Cell temperature: 100 ± 0.01 K
• Ambient diffraction temperature: 100 ± 0.01 K
• Number of distinct elements: 5
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0319
• Residual factor for significantly intense reflections: 0.0293
• Weighted residual factors for significantly intense reflections: 0.0753
• Weighted residual factors for all reflections included in the refinement: 0.077
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No