Information card for entry 7046185

Structure parameters

• Formula: C24 H23 Cl2 Fe N3 Si
• Calculated formula: C24 H23 Cl2 Fe N3 Si
• Title of publication: The coordination chemistry of the neutral tris-2-pyridyl silicon ligand [PhSi(6-Me-2-py)₃].
• Authors of publication: Plajer, Alex J.; Colebatch, Annie L.; Enders, Markus; García-Romero, Álvaro; Bond, Andrew D.; García-Rodríguez, Raúl; Wright, Dominic S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 20
• Pages of publication: 7036 - 7043
• a: 20.9935 ± 0.0005 Å
• b: 10.2893 ± 0.0002 Å
• c: 22.4986 ± 0.0005 Å
• α: 90°
• β: 93.954 ± 0.001°
• γ: 90°
• Cell volume: 4848.32 ± 0.18 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0469
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.0784
• Weighted residual factors for all reflections included in the refinement: 0.0838
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No