Information card for entry 7046358

Structure parameters

• Formula: C85 H89 Mg2 N17
• Calculated formula: C85 H89 Mg2 N17
• Title of publication: 1,4-Dihydropyridyl complexes of magnesium: synthesis by pyridine insertion into the magnesium-silicon bond of triphenylsilyls and catalytic pyridine hydrofunctionalization.
• Authors of publication: Lemmerz, L. E.; Spaniol, T. P.; Okuda, J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 36
• Pages of publication: 12553 - 12561
• a: 21.864 ± 0.004 Å
• b: 11.04 ± 0.002 Å
• c: 32.266 ± 0.005 Å
• α: 90°
• β: 101.021 ± 0.005°
• γ: 90°
• Cell volume: 7645 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.064
• Residual factor for significantly intense reflections: 0.0498
• Weighted residual factors for significantly intense reflections: 0.1223
• Weighted residual factors for all reflections included in the refinement: 0.1306
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No