Information card for entry 7046507

Structure parameters

• Formula: C44 H46 Cl N Ni O3 P2
• Calculated formula: C44 H46 Cl N Ni O3 P2
• Title of publication: Phosphine phosphonic amide nickel catalyzed ethylene polymerization and copolymerization with polar monomers.
• Authors of publication: Hong, Changwen; Sui, Xuelin; Li, Ziqian; Pang, Wenmin; Chen, Min
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 25
• Pages of publication: 8264 - 8267
• a: 17.4215 ± 0.0012 Å
• b: 14.7742 ± 0.0009 Å
• c: 19.0672 ± 0.0015 Å
• α: 90°
• β: 90.882 ± 0.002°
• γ: 90°
• Cell volume: 4907.1 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1399
• Residual factor for significantly intense reflections: 0.068
• Weighted residual factors for significantly intense reflections: 0.1038
• Weighted residual factors for all reflections included in the refinement: 0.1175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No