Information card for entry 7046555

Structure parameters

• Formula: C82 H46 B2 F30 N2 O2 P2
• Calculated formula: C82 H46 B2 F30 N2 O2 P2
• Title of publication: Interception of intermediates in phosphine oxidation by mesityl nitrile-N-oxide using frustrated Lewis pairs.
• Authors of publication: Szkop, Kevin M.; Zhu, Diya; Longobardi, Lauren E.; Heck, Julian; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 27
• Pages of publication: 8933 - 8939
• a: 11.6128 ± 0.0017 Å
• b: 11.9186 ± 0.0018 Å
• c: 15.044 ± 0.002 Å
• α: 94.439 ± 0.005°
• β: 108.206 ± 0.004°
• γ: 111.791 ± 0.004°
• Cell volume: 1792 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0855
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.0903
• Weighted residual factors for all reflections included in the refinement: 0.1055
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No