Information card for entry 7046587

Structure parameters

• Formula: C31 H19 F18 Gd N2 O9
• Calculated formula: C30.9999 H18.9995 F18 Gd N2 O9
• Title of publication: The modular synthesis of rare earth-transition metal heterobimetallic complexes utilizing a redox-active ligand.
• Authors of publication: Hickson, James R.; Horsewill, Samuel J.; Bamforth, Christopher; McGuire, Jake; Wilson, Claire; Sproules, Stephen; Farnaby, Joy H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 31
• Pages of publication: 10692 - 10701
• a: 9.62 ± 0.0003 Å
• b: 22.9967 ± 0.0006 Å
• c: 17.1078 ± 0.0004 Å
• α: 90°
• β: 98.929 ± 0.002°
• γ: 90°
• Cell volume: 3738.86 ± 0.18 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1014
• Residual factor for significantly intense reflections: 0.0915
• Weighted residual factors for significantly intense reflections: 0.2707
• Weighted residual factors for all reflections included in the refinement: 0.2793
• Goodness-of-fit parameter for all reflections included in the refinement: 1.13
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No