Information card for entry 7046635

Structure parameters

• Formula: C19 H37 Cl2 N2 Ni O P
• Calculated formula: C19 H37 Cl2 N2 Ni O P
• Title of publication: Electrocatalytic proton reduction by an air-stable nickel(ii)-thiolato PNN pincer complex.
• Authors of publication: Yap, Chew Pheng; Chong, Yuan Yi; Chwee, Tsz Sian; Fan, Wai Yip
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 25
• Pages of publication: 8483 - 8488
• a: 31.456 ± 0.005 Å
• b: 10.5339 ± 0.0017 Å
• c: 13.821 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4579.6 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0356
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.0717
• Weighted residual factors for all reflections included in the refinement: 0.0731
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No