Crystallography Open Database

Information card for entry 7046665

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Coordinates	7046665.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H74 Ca2 K2 N2 O2 Si4
Calculated formula	C42 H74 Ca2 K2 N2 O2 Si4
Title of publication	Cyclooctatetraenyl calcium and strontium amido complexes.
Authors of publication	Sroor, Farid M.; Vendier, Laure; Etienne, Michel
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	36
Pages of publication	12587 - 12595
a	25.3493 ± 0.0019 Å
b	11.5675 ± 0.0008 Å
c	17.5984 ± 0.0013 Å
α	90°
β	96.128 ± 0.002°
γ	90°
Cell volume	5130.9 ± 0.6 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0465
Residual factor for significantly intense reflections	0.0437
Weighted residual factors for significantly intense reflections	0.1064
Weighted residual factors for all reflections included in the refinement	0.1087
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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