Information card for entry 7046667

Structure parameters

• Formula: C21 H34 Ca K N Si2
• Calculated formula: C21 H34 Ca K N Si2
• Title of publication: Cyclooctatetraenyl calcium and strontium amido complexes.
• Authors of publication: Sroor, Farid M.; Vendier, Laure; Etienne, Michel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 36
• Pages of publication: 12587 - 12595
• a: 14.7841 ± 0.0006 Å
• b: 10.8936 ± 0.0004 Å
• c: 15.0864 ± 0.0006 Å
• α: 90°
• β: 103.63 ± 0.001°
• γ: 90°
• Cell volume: 2361.27 ± 0.16 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0829
• Residual factor for significantly intense reflections: 0.0557
• Weighted residual factors for all reflections: 0.0949
• Weighted residual factors for significantly intense reflections: 0.0532
• Weighted residual factors for all reflections included in the refinement: 0.0504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0556
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No