Information card for entry 7046682

Structure parameters

• Formula: C27 H30 Cl2 F6 O P Rh
• Calculated formula: C27 H30 Cl2 F6 O P Rh
• Title of publication: Rhodafuran from a methoxy(alkenyl)carbene by the rhoda-1,3,5-hexatriene route.
• Authors of publication: Talavera, M.; Pereira-Cameselle, R; Bolaño, S
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 27
• Pages of publication: 9064 - 9071
• a: 13.2268 ± 0.0007 Å
• b: 13.8277 ± 0.0008 Å
• c: 16.2267 ± 0.001 Å
• α: 93.287 ± 0.002°
• β: 96 ± 0.002°
• γ: 110.135 ± 0.002°
• Cell volume: 2757.3 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0617
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.0811
• Weighted residual factors for all reflections included in the refinement: 0.0849
• Goodness-of-fit parameter for all reflections included in the refinement: 1.139
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No