Information card for entry 7046854

Structure parameters

• Formula: C68 H92 Fe4 N8 P4
• Calculated formula: C68 H92 Fe4 N8 P4
• Title of publication: Redox behaviour of ([fc(NPⁱPr₂)₂]Fe)₂, formation of an iron-iron bond and cleavage of azobenzene.
• Authors of publication: Pick, Fraser S.; Leznoff, Daniel B.; Fryzuk, Michael D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 32
• Pages of publication: 10925 - 10931
• a: 13.6777 ± 0.0007 Å
• b: 13.5134 ± 0.0006 Å
• c: 17.7979 ± 0.0008 Å
• α: 90°
• β: 94.014 ± 0.001°
• γ: 90°
• Cell volume: 3281.6 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0372
• Residual factor for significantly intense reflections: 0.0279
• Weighted residual factors for significantly intense reflections: 0.0638
• Weighted residual factors for all reflections included in the refinement: 0.0675
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No