Information card for entry 7046862

Structure parameters

• Formula: C29 H75 Co4 F15 Mo4 N12 O38 S5
• Calculated formula: C29 H63 Co4 F15 Mo4 N12 O38.001 S5
• Title of publication: Synthesis of cationic molybdenum-cobalt heterometallic clusters protected against hydrolysis by macrocyclic triazacyclononane complexes.
• Authors of publication: Sugiarto, ?; Tagami, Tomoko; Kawamoto, Keisuke; Hayashi, Yoshihito
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 29
• Pages of publication: 9657 - 9664
• a: 23.1839 ± 0.0005 Å
• b: 18.5915 ± 0.0004 Å
• c: 16.4545 ± 0.0003 Å
• α: 90°
• β: 90.69 ± 0.01°
• γ: 90°
• Cell volume: 7091.8 ± 0.3 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0916
• Residual factor for significantly intense reflections: 0.0647
• Weighted residual factors for significantly intense reflections: 0.1402
• Weighted residual factors for all reflections included in the refinement: 0.1538
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No