Information card for entry 7046942

Structure parameters

• Formula: C40 H72 Cl Mo N4 P3
• Calculated formula: C40 H72 Cl Mo N4 P3
• Title of publication: The new diphosphanylphosphido complexes of tungsten(vi) and molybdenum(vi). Their synthesis, structures and properties.
• Authors of publication: Wiśniewska, A; Grubba, R.; Ponikiewski, Ł; Zauliczny, M.; Pikies, J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 30
• Pages of publication: 10213 - 10222
• a: 11.0012 ± 0.001 Å
• b: 20.8791 ± 0.0014 Å
• c: 22.0534 ± 0.0014 Å
• α: 105.878 ± 0.005°
• β: 102.963 ± 0.006°
• γ: 102.3 ± 0.007°
• Cell volume: 4540.1 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0564
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1089
• Weighted residual factors for all reflections included in the refinement: 0.1162
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No