Information card for entry 7047085

Structure parameters

• Formula: C24 H9 F20 P
• Calculated formula: C24 H9 F20 P
• Title of publication: Probing steric influences on electrophilic phosphonium cations: a comparison of [(3,5-(CF₃)₂C₆H₃)₃PF]⁺ and [(C₆F₅)₃PF]<sup/>.
• Authors of publication: LaFortune, James H. W.; Szkop, Kevin M.; Farinha, Farah E.; Johnstone, Timothy C.; Postle, Shawn; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 33
• Pages of publication: 11411 - 11419
• a: 8.911 ± 0.004 Å
• b: 9.461 ± 0.004 Å
• c: 14.845 ± 0.006 Å
• α: 90°
• β: 100.447 ± 0.014°
• γ: 90°
• Cell volume: 1230.8 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0658
• Residual factor for significantly intense reflections: 0.0547
• Weighted residual factors for significantly intense reflections: 0.1563
• Weighted residual factors for all reflections included in the refinement: 0.1851
• Goodness-of-fit parameter for all reflections included in the refinement: 1.145
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No