Information card for entry 7047142

Structure parameters

• Formula: C33 H36 N O P Rh Sb
• Calculated formula: C33 H36 N O P Rh Sb
• Title of publication: Synthesis and characterization of rhodium, iridium, and palladium complexes of a diarylamido-based PNSb pincer ligand.
• Authors of publication: Kosanovich, Alex J.; Jordan, Aldo M.; Bhuvanesh, Nattamai; Ozerov, Oleg V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 33
• Pages of publication: 11619 - 11624
• a: 10.5285 ± 0.0002 Å
• b: 14.0615 ± 0.0003 Å
• c: 20.1189 ± 0.0004 Å
• α: 90°
• β: 92.004 ± 0.001°
• γ: 90°
• Cell volume: 2976.71 ± 0.1 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0416
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0673
• Weighted residual factors for all reflections included in the refinement: 0.073
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No