Information card for entry 7047383

Structure parameters

• Formula: C37 H56 Cl N5 Pd
• Calculated formula: C37 H56 Cl N5 Pd
• Title of publication: Palladium alkyl complexes with a formazanate ligand: synthesis, structure and reactivity.
• Authors of publication: Milocco, Francesca; de Vries, Folkert; Dall'Anese, Anna; Rosar, Vera; Zangrando, Ennio; Otten, Edwin; Milani, Barbara
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 41
• Pages of publication: 14445 - 14451
• a: 14.8027 ± 0.0006 Å
• b: 16.6849 ± 0.0006 Å
• c: 15.6639 ± 0.0006 Å
• α: 90°
• β: 107.675 ± 0.002°
• γ: 90°
• Cell volume: 3686.1 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0749
• Residual factor for significantly intense reflections: 0.057
• Weighted residual factors for significantly intense reflections: 0.1056
• Weighted residual factors for all reflections included in the refinement: 0.1199
• Goodness-of-fit parameter for all reflections included in the refinement: 1.197
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No