Information card for entry 7047576

Structure parameters

• Formula: C34 H58 N4 Ni O P2
• Calculated formula: C34 H58 N4 Ni O P2
• Title of publication: Monomeric nickel hydroxide stabilized by a sterically demanding phosphorus-nitrogen PN³P-pincer ligand: synthesis, reactivity and catalysis.
• Authors of publication: Yao, Changguang; Chakraborty, Priyanka; Aresu, Emanuele; Li, Huaifeng; Guan, Chao; Zhou, Chunhui; Liang, Lan-Chang; Huang, Kuo-Wei
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 45
• Pages of publication: 16057 - 16065
• a: 8.821 ± 0.003 Å
• b: 27.389 ± 0.008 Å
• c: 15.683 ± 0.005 Å
• α: 90°
• β: 106.055 ± 0.013°
• γ: 90°
• Cell volume: 3641 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0956
• Residual factor for significantly intense reflections: 0.0593
• Weighted residual factors for significantly intense reflections: 0.1535
• Weighted residual factors for all reflections included in the refinement: 0.174
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No