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Information card for entry 7047627
Preview
Coordinates | 7047627.cif |
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Original paper (by DOI) | HTML |
Formula | C46 H36 Cl2 Fe2 N2 P2 Pd |
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Calculated formula | C46 H36 Cl2 Fe2 N2 P2 Pd |
Title of publication | Comparing the reactivity of isomeric phosphinoferrocene nitrile and isocyanide in Pd(ii) complexes: synthesis of simple coordination compounds vs. preparation of P-chelated insertion products and Fischer-type carbenes. |
Authors of publication | Škoch, Karel; Císařová, Ivana; Uhlík, Filip; Štěpnička, Petr |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2018 |
Journal volume | 47 |
Journal issue | 45 |
Pages of publication | 16082 - 16101 |
a | 8.9445 ± 0.0004 Å |
b | 10.066 ± 0.0004 Å |
c | 11.2913 ± 0.0004 Å |
α | 82.15 ± 0.002° |
β | 74.759 ± 0.002° |
γ | 85.368 ± 0.002° |
Cell volume | 970.6 ± 0.07 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0396 |
Residual factor for significantly intense reflections | 0.029 |
Weighted residual factors for significantly intense reflections | 0.0572 |
Weighted residual factors for all reflections included in the refinement | 0.0607 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.038 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7047627.html
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