Information card for entry 7047656

Structure parameters

• Formula: C32 H47 N S U
• Calculated formula: C32.009 H29 N S1.3886 U
• Title of publication: A sulphur and uranium fiesta! Synthesis, structure, and characterization of neutral terminal uranium(vi) monosulphide, uranium(vi) η²-disulphide, and uranium(iv) phosphine sulphide complexes.
• Authors of publication: Pagano, Justin K.; Arney, David S. J.; Scott, Brian L.; Morris, David E.; Kiplinger, Jaqueline L.; Burns, Carol J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 48
• Journal issue: 1
• Pages of publication: 50 - 57
• a: 31.606 ± 0.002 Å
• b: 10.2542 ± 0.0007 Å
• c: 18.4969 ± 0.0013 Å
• α: 90°
• β: 92.8494 ± 0.0015°
• γ: 90°
• Cell volume: 5987.3 ± 0.7 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0454
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0861
• Weighted residual factors for all reflections included in the refinement: 0.0922
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No