Mononuclear iron(ii) complexes containing a tripodal and macrocyclic nitrogen ligand: synthesis, reactivity and application in cyclohexane oxidation catalysis.
Authors of publication
Ayad, Massinisa; Klein Gebbink, Robertus J. M.; Le Mest, Yves; Schollhammer, Philippe; Le Poul, Nicolas; Pétillon, François Y; Mandon, Dominique
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2018
Journal volume
47
Journal issue
43
Pages of publication
15596 - 15612
a
11.6048 ± 0.0004 Å
b
13.6563 ± 0.0006 Å
c
14.1144 ± 0.0004 Å
α
116.401 ± 0.004°
β
92.178 ± 0.003°
γ
109.682 ± 0.004°
Cell volume
1839.14 ± 0.16 Å3
Cell temperature
170 ± 2 K
Ambient diffraction temperature
170 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0524
Residual factor for significantly intense reflections
0.0396
Weighted residual factors for significantly intense reflections
0.0982
Weighted residual factors for all reflections included in the refinement
0.106
Goodness-of-fit parameter for all reflections included in the refinement
