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Information card for entry 7047732
Preview
Coordinates | 7047732.cif |
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Original paper (by DOI) | HTML |
Formula | C33 H58 Cl2 Ge N2 O Rh Si2 |
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Calculated formula | C33 H58 Cl2 Ge N2 O Rh Si2 |
Title of publication | Cyclometallation of a germylene ligand by concerted metalation-deprotonation of a methyl group. |
Authors of publication | Bakthavachalam, K.; Dutta, Sayan; C, Arivazhagan; Raghavendra, Beesam; Haridas, Anagha; Sen, Sakya S.; Koley, Debasis; Ghosh, Sundargopal |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2018 |
Journal volume | 47 |
Journal issue | 44 |
Pages of publication | 15835 - 15844 |
a | 43.1777 ± 0.0013 Å |
b | 31.7106 ± 0.0009 Å |
c | 12.5293 ± 0.0003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 17155 ± 0.8 Å3 |
Cell temperature | 247 ± 40 K |
Ambient diffraction temperature | 247 ± 40 K |
Number of distinct elements | 8 |
Space group number | 43 |
Hermann-Mauguin space group symbol | F d d 2 |
Hall space group symbol | F 2 -2d |
Residual factor for all reflections | 0.0423 |
Residual factor for significantly intense reflections | 0.0357 |
Weighted residual factors for significantly intense reflections | 0.0962 |
Weighted residual factors for all reflections included in the refinement | 0.1011 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.072 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7047732.html
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