Information card for entry 7047763

Structure parameters

• Formula: C25 H50 Be6 Cl6 O16
• Calculated formula: C24 H48 Be6 Cl4 O16
• Title of publication: The coordination behaviour and reactivity of partially silicon based crown ethers towards beryllium chloride.
• Authors of publication: Buchner, Magnus R.; Müller, Matthias; Dankert, Fabian; Reuter, Kirsten; von Hänisch, Carsten
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 46
• Pages of publication: 16393 - 16397
• a: 19.481 ± 0.004 Å
• b: 9.5492 ± 0.0019 Å
• c: 21.762 ± 0.004 Å
• α: 90°
• β: 106.72 ± 0.03°
• γ: 90°
• Cell volume: 3877.2 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0636
• Residual factor for significantly intense reflections: 0.0525
• Weighted residual factors for significantly intense reflections: 0.1403
• Weighted residual factors for all reflections included in the refinement: 0.1482
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No