Information card for entry 7047871

Structure parameters

• Formula: C54 H86 F4 O20 Rh4
• Calculated formula: C54 H86 F4 O20 Rh4
• Title of publication: Experimental and theoretical study of dimer-of-dimers-type tetrarhodium(ii) complexes bridged by 1,4-benzenedicarboxylate linkers.
• Authors of publication: Kataoka, Yusuke; Arakawa, Kazuki; Ueda, Hikaru; Yano, Natsumi; Kawamoto, Tatsuya; Handa, Makoto
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 48
• Pages of publication: 17233 - 17242
• a: 11.5391 ± 0.0018 Å
• b: 17.587 ± 0.002 Å
• c: 16.956 ± 0.003 Å
• α: 90°
• β: 109.225 ± 0.003°
• γ: 90°
• Cell volume: 3249.1 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0321
• Residual factor for significantly intense reflections: 0.0297
• Weighted residual factors for significantly intense reflections: 0.0708
• Weighted residual factors for all reflections included in the refinement: 0.0731
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No