Information card for entry 7047959

Structure parameters

• Formula: C54 H64 Ge N4 O4
• Calculated formula: C54 H64 Ge N4 O4
• Title of publication: Halogen-free GeO₂ conversion: electrochemical reduction vs. complexation in (DTBC)₂Ge[Py(CN)_n] (n = 0…2) complexes.
• Authors of publication: Nikolaevskaya, Elena N.; Saverina, Evgeniya A.; Starikova, Alyona A.; Farhati, Amel; Kiskin, Mikhail A.; Syroeshkin, Mikhail A.; Egorov, Mikhail P.; Jouikov, Viatcheslav V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 47
• Pages of publication: 17127 - 17133
• a: 15.0823 ± 0.0015 Å
• b: 22.183 ± 0.002 Å
• c: 7.363 ± 0.0008 Å
• α: 90°
• β: 94.243 ± 0.002°
• γ: 90°
• Cell volume: 2456.7 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.101
• Residual factor for significantly intense reflections: 0.0513
• Weighted residual factors for significantly intense reflections: 0.1246
• Weighted residual factors for all reflections included in the refinement: 0.1605
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No