Information card for entry 7047971

Structure parameters

• Formula: C24 H29 N P2
• Calculated formula: C24 H29 N P2
• Title of publication: Symmetrical and unsymmetrical diphosphanes with diversified alkyl, aryl, and amino substituents.
• Authors of publication: Szynkiewicz, Natalia; Ponikiewski, Łukasz; Grubba, Rafał
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 47
• Pages of publication: 16885 - 16894
• a: 37.194 ± 0.002 Å
• b: 8.2421 ± 0.0004 Å
• c: 15.7504 ± 0.0009 Å
• α: 90°
• β: 113.193 ± 0.004°
• γ: 90°
• Cell volume: 4438.2 ± 0.4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1032
• Residual factor for significantly intense reflections: 0.077
• Weighted residual factors for significantly intense reflections: 0.2279
• Weighted residual factors for all reflections included in the refinement: 0.2517
• Goodness-of-fit parameter for all reflections included in the refinement: 1.138
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No