Crystallography Open Database

Information card for entry 7047982

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Coordinates	7047982.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H33 N P2
Calculated formula	C22 H33 N P2
Title of publication	Symmetrical and unsymmetrical diphosphanes with diversified alkyl, aryl, and amino substituents.
Authors of publication	Szynkiewicz, Natalia; Ponikiewski, Łukasz; Grubba, Rafał
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	47
Pages of publication	16885 - 16894
a	9.3935 ± 0.0005 Å
b	11.1597 ± 0.0006 Å
c	11.2752 ± 0.0006 Å
α	110.014 ± 0.004°
β	100.623 ± 0.004°
γ	95.397 ± 0.004°
Cell volume	1075.63 ± 0.11 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0801
Residual factor for significantly intense reflections	0.0637
Weighted residual factors for significantly intense reflections	0.1669
Weighted residual factors for all reflections included in the refinement	0.1784
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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