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Information card for entry 7048076
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Coordinates | 7048076.cif |
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Original paper (by DOI) | HTML |
Formula | C60 H100 K2 O15 Tb |
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Calculated formula | C60 H100 K2 O15 Tb |
Title of publication | Isolation of reactive Ln(ii) complexes with C<sub>5</sub>H<sub>4</sub>Me ligands (Cp<sup>Me</sup>) using inverse sandwich countercations: synthesis and structure of [(18-crown-6)K(μ-Cp<sup>Me</sup>)K(18-crown-6)][Cp<sup>Me</sup><sub>3</sub>Ln<sup>II</sup>] (Ln = Tb, Ho). |
Authors of publication | Huh, Daniel N.; Ziller, Joseph W.; Evans, William J. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2018 |
Journal volume | 47 |
Journal issue | 48 |
Pages of publication | 17285 - 17290 |
a | 9.593 ± 0.003 Å |
b | 26.141 ± 0.009 Å |
c | 25.231 ± 0.008 Å |
α | 90° |
β | 90.774 ± 0.004° |
γ | 90° |
Cell volume | 6327 ± 4 Å3 |
Cell temperature | 133 ± 2 K |
Ambient diffraction temperature | 133 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0565 |
Residual factor for significantly intense reflections | 0.0389 |
Weighted residual factors for significantly intense reflections | 0.0886 |
Weighted residual factors for all reflections included in the refinement | 0.0959 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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